Technology Process of C24H29FN6O2Si
There total 4 articles about C24H29FN6O2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium permanganate; water; sodium hydrogencarbonate; magnesium sulfate / acetone
2: water; sodium carbonate / 1,4-dioxane; ethanol
3: tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water
With
potassium permanganate; tetrakis(triphenylphosphine) palladium(0); water; sodium hydrogencarbonate; sodium carbonate; magnesium sulfate;
In
1,4-dioxane; ethanol; water; acetone;
3: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.07.057
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; sodium carbonate / 1,4-dioxane; ethanol
2: tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water
With
tetrakis(triphenylphosphine) palladium(0); water; sodium carbonate;
In
1,4-dioxane; ethanol; water;
2: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.07.057
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide
2: potassium permanganate; water; sodium hydrogencarbonate; magnesium sulfate / acetone
3: water; sodium carbonate / 1,4-dioxane; ethanol
4: tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water
With
bis-triphenylphosphine-palladium(II) chloride; potassium permanganate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); water; sodium hydrogencarbonate; sodium carbonate; magnesium sulfate; triethylamine;
In
1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; acetone;
1: Sonogashira coupling / 4: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.07.057