dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate

Base Information

Chemical Name:dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate
CAS No.:1455471-53-0
Molecular Formula:C₁₂H₁₅NO₄
Molecular Weight:237.255
Hs Code.:

Synonyms:

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Chemical Property of dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate

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Technology Process of dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate

There total 5 articles about dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 192508-36-4
2-(4-fluoro-3-nitrophenyl)acetic acid

: 1455471-53-0
dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / ethanol / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

3: hydrogenchloride / water / 120 °C

4: hydrogen; palladium 10% on activated carbon / 16 h / 20 °C

With hydrogenchloride; thionyl chloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1455471-50-7
diethyl 2-(4-(2-ethoxy-2-oxoethyl)-2-nitrophenyl)malonate

: 1455471-53-0
dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 120 °C

2: hydrogen; palladium 10% on activated carbon / 16 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In water;

Reference yield:

: 405-50-5
p-Fluorophenylacetic acid

: 1455471-53-0
dimethyl 2,2'-(2-amino-1,4-phenylene)diacetate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; potassium nitrate / 1.5 h / 0 °C

2: thionyl chloride / ethanol / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

4: hydrogenchloride / water / 120 °C

5: hydrogen; palladium 10% on activated carbon / 16 h / 20 °C

With hydrogenchloride; thionyl chloride; potassium nitrate; sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;