Technology Process of 5-(4-methoxyphenyl)-5-oxo-2,2-diphenylpentanoic acid
There total 3 articles about 5-(4-methoxyphenyl)-5-oxo-2,2-diphenylpentanoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) sodium ethoxide / 1.) EtOH, 5 min. reflux, 2.) room temperature, 1,5 h
2: KOH / aq. ethanol / 6 h / Heating
3: 81 percent / acetic anhydride / 2 h / Heating
4: 64 percent / AlCl3 / nitrobenzene / 6 h / Ambient temperature
With
potassium hydroxide; aluminium trichloride; sodium ethanolate; acetic anhydride;
In
ethanol; nitrobenzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 81 percent / acetic anhydride / 2 h / Heating
2: 64 percent / AlCl3 / nitrobenzene / 6 h / Ambient temperature
With
aluminium trichloride; acetic anhydride;
In
nitrobenzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: KOH / aq. ethanol / 6 h / Heating
2: 81 percent / acetic anhydride / 2 h / Heating
3: 64 percent / AlCl3 / nitrobenzene / 6 h / Ambient temperature
With
potassium hydroxide; aluminium trichloride; acetic anhydride;
In
ethanol; nitrobenzene;