hexaazatriphenylenehexacarboxylic acid trianhydride

Base Information

Chemical Name:hexaazatriphenylenehexacarboxylic acid trianhydride
CAS No.:105618-29-9
Molecular Formula:C₁₈N₆O₉
Molecular Weight:444.233
Hs Code.:

Synonyms:

Suppliers and Price of hexaazatriphenylenehexacarboxylic acid trianhydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of hexaazatriphenylenehexacarboxylic acid trianhydride

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of hexaazatriphenylenehexacarboxylic acid trianhydride

There total 4 articles about hexaazatriphenylenehexacarboxylic acid trianhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 105598-29-6
hexaazatriphenylenehexacarboxylic acid

: 105618-29-9
hexaazatriphenylenehexacarboxylic acid trianhydride

Guidance literature:: With acetic anhydride; at 115 ℃; for 0.166667h;
DOI:10.1021/jo00376a036

Reference yield:

: 527-31-1
hexaketocyclohexane

: 105618-29-9
hexaazatriphenylenehexacarboxylic acid trianhydride

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / 2 h / Reflux

2.1: sulfuric acid / 72 h / 20 °C

3.1: acetic acid; sodium nitrite; trifluoroacetic acid / 12 h

3.2: 12 h / 20 °C

4.1: acetic anhydride / 0.33 h / 115 - 117 °C / Inert atmosphere

With sulfuric acid; acetic anhydride; acetic acid; trifluoroacetic acid; sodium nitrite;
DOI:10.1039/c8nj03793k

Reference yield:

: 105598-27-4
dipyrazino[2,3-f:20,30-h]quinoxaline-2,3,6,7,10,11-hexacarbonitrile

: 105618-29-9
hexaazatriphenylenehexacarboxylic acid trianhydride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 72 h / 20 °C

2.1: acetic acid; sodium nitrite; trifluoroacetic acid / 12 h

2.2: 12 h / 20 °C

3.1: acetic anhydride / 0.33 h / 115 - 117 °C / Inert atmosphere

With sulfuric acid; acetic anhydride; acetic acid; trifluoroacetic acid; sodium nitrite;
DOI:10.1039/c8nj03793k