Technology Process of C26H38F2N2O4
There total 11 articles about C26H38F2N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: n-butyllithium / tetrahydrofuran / -78 °C
2: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C
3: hydrogenchloride / methanol / 20 °C
4: triethylamine / dichloromethane / 20 °C
5: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C
6: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C
7: chloro-trimethyl-silane / dichloromethane / 20 °C
8: palladium 10% on activated carbon; hydrogen / ethanol
9: Decaborane / methanol / 20 °C
With
hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; Decaborane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
6: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogenchloride / methanol / 20 °C
2: triethylamine / dichloromethane / 20 °C
3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C
4: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C
5: chloro-trimethyl-silane / dichloromethane / 20 °C
6: palladium 10% on activated carbon; hydrogen / ethanol
7: Decaborane / methanol / 20 °C
With
hydrogenchloride; chloro-trimethyl-silane; Decaborane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060