Technology Process of Ethyl pyruvate 2-(2-methoxyphenyl)phenylhydrazone
There total 6 articles about Ethyl pyruvate 2-(2-methoxyphenyl)phenylhydrazone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid;
In
ethanol;
for 0.0833333h;
Heating;
DOI:10.1248/cpb.39.572
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 81 percent / K2CO3, Cu-powder, I2 / nitrobenzene / 34 h / Heating
2: 97 percent / 40percent H2SO4 / 10 h / Heating
3: 93 percent / NaNO2, conc. HCl / H2O / 1 h / 0 - 4 °C
4: 5.955 g / Zn powder, AcOH, H2O / 10 h / ice-cooling
5: 45 percent / AcOH / ethanol / 0.08 h / Heating
With
hydrogenchloride; sulfuric acid; water; iodine; copper; potassium carbonate; acetic acid; zinc; sodium nitrite;
In
ethanol; water; nitrobenzene;
DOI:10.1248/cpb.39.572
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 81 percent / K2CO3, Cu-powder, I2 / nitrobenzene / 34 h / Heating
2: 97 percent / 40percent H2SO4 / 10 h / Heating
3: 93 percent / NaNO2, conc. HCl / H2O / 1 h / 0 - 4 °C
4: 5.955 g / Zn powder, AcOH, H2O / 10 h / ice-cooling
5: 45 percent / AcOH / ethanol / 0.08 h / Heating
With
hydrogenchloride; sulfuric acid; water; iodine; copper; potassium carbonate; acetic acid; zinc; sodium nitrite;
In
ethanol; water; nitrobenzene;
DOI:10.1248/cpb.39.572
