1D-O⁴-(6-amino-2,3-azanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O⁶-(2,3-diamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-2-deoxy-streptamine

Base Information

• Chemical Name: 1D-O⁴-(6-amino-2,3-azanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O⁶-(2,3-diamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-2-deoxy-streptamine
• CAS No.: 70038-42-5
• Molecular Formula: C₁₈H₃₆N₆O₆
• Molecular Weight: 432.52

Synonyms:

Chemical Property of 1D-O⁴-(6-amino-2,3-azanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O⁶-(2,3-diamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-2-deoxy-streptamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1D-O⁴-(6-amino-2,3-azanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O⁶-(2,3-diamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-2-deoxy-streptamine

There total 2 articles about 1D-O⁴-(6-amino-2,3-azanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O⁶-(2,3-diamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-2-deoxy-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1L-O4-(2,3-bis-ethoxycarbonylamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-O6-[2,6-bis-ethoxycarbonylamino-O3-(toluene-4-sulfonyl)-α-D-xylo-2,4,6-trideoxy-hexopyranosyl]-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine (64960-98-1) → 1D-O4-(6-amino-2,3-azanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O6-(2,3-diamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-2-deoxy-streptamine (70038-42-5)

Guidance literature:

Multi-step reaction with 3 steps

1: NaBH₄ / dimethylsulfoxide

2: aq. Na₂CO₃ / dimethylformamide

3: aq. KOH / methanol

With potassium hydroxide; sodium tetrahydroborate; sodium carbonate; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1246/bcsj.51.3553

Reference yield:

1D-O4-(2,3-azanediyl-6-ethoxycarbonylamino-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O6-(2,3-bis-ethoxycarbonylamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine (68594-13-8) → 1D-O4-(6-amino-2,3-azanediyl-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O6-(2,3-diamino-O4-methyl-α-D-2,3-dideoxy-xylopyranosyl)-2-deoxy-streptamine (70038-42-5)

Guidance literature:

With potassium hydroxide; In methanol;

DOI:10.1246/bcsj.51.3553

upstream raw materials:

1D-O⁴-(2,3-azanediyl-6-ethoxycarbonylamino-α-D-ribo-2,3,4,6-tetradeoxy-hexopyranosyl)-O⁶-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine

1L-O⁴-(2,3-bis-ethoxycarbonylamino-O⁴-methyl-α-D-2,3-dideoxy-xylopyranosyl)-O⁶-[2,6-bis-ethoxycarbonylamino-O³-(toluene-4-sulfonyl)-α-D-xylo-2,4,6-trideoxy-hexopyranosyl]-N,N'-bis-ethoxycarbonyl-2-deoxy-streptamine

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