5-amino-2-cyclopentyl-4-methylphenol

Base Information

Chemical Name:5-amino-2-cyclopentyl-4-methylphenol
CAS No.:1161025-14-4
Molecular Formula:C₁₂H₁₇NO
Molecular Weight:191.273
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-amino-2-cyclopentyl-4-methylphenol

Chemical Property:

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Technology Process of 5-amino-2-cyclopentyl-4-methylphenol

There total 4 articles about 5-amino-2-cyclopentyl-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55910-44-6
4-bromo-2-cyclopentylphenol

: 1161025-14-4
5-amino-2-cyclopentyl-4-methylphenol

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dmap / dichloromethane / 2 h / 0 - 20 °C

2: sulfuric acid; nitric acid / 1 h / -10 °C

3: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 0.58 h / 110 °C / Microwave irradiation

4: hydrogen / palladium 10% on activated carbon / methanol / 4 h / Heating / reflux

With sulfuric acid; hydrogen; nitric acid; caesium carbonate; triethylamine; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 1161025-10-0
4-bromo-2-cyclopentyl-5-nitrophenyl methyl carbonate

: 1161025-14-4
5-amino-2-cyclopentyl-4-methylphenol

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 0.58 h / 110 °C / Microwave irradiation

2: hydrogen / palladium 10% on activated carbon / methanol / 4 h / Heating / reflux

With hydrogen; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; water;

Reference yield:

: 1518-84-9
2-cyclopentylphenol

: 1161025-14-4
5-amino-2-cyclopentyl-4-methylphenol

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen bromide; acetic acid; dimethyl sulfoxide / water / 0.17 h

2: triethylamine / dmap / dichloromethane / 2 h / 0 - 20 °C

3: sulfuric acid; nitric acid / 1 h / -10 °C

4: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 0.58 h / 110 °C / Microwave irradiation

5: hydrogen / palladium 10% on activated carbon / methanol / 4 h / Heating / reflux

With sulfuric acid; hydrogen bromide; hydrogen; nitric acid; caesium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water;