2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

• Chemical Name: 2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside
• CAS No.: 1007126-84-2
• Molecular Formula: C₃₅H₄₅F₃N₂O₁₇
• Molecular Weight: 822.741
• Mol file: 1007126-84-2.mol

Synonyms:

Chemical Property of 2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 1 articles about 2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C33H43F3N2O16 + acetic anhydride (108-24-7) → 2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside (1007126-84-2)

Guidance literature:

With pyridine;

DOI:10.1134/S1068162007010141

Reference yield:

2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside (1007126-84-2) + acetic anhydride (108-24-7) + Triethyl orthoacetate (78-39-7) → C34H45F3N2O16

Guidance literature:

2-(trifluoroacetamido)ethyl 2-acetamido-3,6-di-O-acetyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside; With sodium methylate; In methanol;

Triethyl orthoacetate; With toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; for 1h;

acetic anhydride; With pyridine; Further stages.;

DOI:10.1134/S1068162007010141

upstream raw materials:

acetic anhydride