diiodotetrakis(triphenylarsine oxide)hexaiodouranate(IV)

Base Information

• Chemical Name: diiodotetrakis(triphenylarsine oxide)hexaiodouranate(IV)
• CAS No.: 110305-48-1
• Molecular Formula: C₇₂H₆₀As₄I₂O₄U*I₆U
• Molecular Weight: 2780.25

Synonyms:

Chemical Property of diiodotetrakis(triphenylarsine oxide)hexaiodouranate(IV)

Chemical Property:

Purity/Quality:

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Technology Process of diiodotetrakis(triphenylarsine oxide)hexaiodouranate(IV)

There total 5 articles about diiodotetrakis(triphenylarsine oxide)hexaiodouranate(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[UI4(acetonitrile)4] + triphenylarsineoxide (1153-05-5,856568-31-5) → diiodotetrakis(triphenylarsine oxide)hexaiodouranate(IV) (110305-48-1)

Guidance literature:

With Bu₄NI; In dichloromethane; ethyl acetate; acetonitrile; to a soln. of the U complex in MeCO2Et is added 2 equiv of Bu4NI in a min. of MeCN, followed by 2 equiv of Ph3AsO (from stock soln. in CH2Cl2); ppt. washed with isopentane (1x5 ml), dried in vac.; elem. anal.;

DOI:10.1016/S0020-1693(00)88101-3

Reference yield:

UI4(triphenylarsine oxide)2 → di-iodotetrakis(triphenylarsine oxide)uranium(IV) hexaiodouranate(IV) (110305-48-1)

Guidance literature:

In ethyl acetate; acetonitrile; suspn. in CH3CN/ethyl acetate;;

DOI:10.1016/S0020-1693(00)84049-9

Reference yield:

uranium tetraiodide (13470-22-9) + triphenylarsineoxide (1153-05-5,856568-31-5) → diiodotetrakis(triphenylarsine oxide)hexaiodouranate(IV) (110305-48-1)

Guidance literature:

In ethyl acetate; acetonitrile; at room temp.; 2 equiv of Ph3AsO; elem. anal.;

DOI:10.1016/S0020-1693(00)88101-3

upstream raw materials:

UI₄(CH₃CN)4

triphenylarsineoxide

uranium tetraiodide

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