N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine

Base Information

Chemical Name:N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine
CAS No.:129819-55-2
Molecular Formula:C₂₁H₂₃NO₂S
Molecular Weight:353.485
Hs Code.:

Synonyms:

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Chemical Property of N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine

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Technology Process of N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine

There total 10 articles about N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 129819-55-2
N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / ZnCl₂ / acetic acid / 3 h / 60 °C

2: 88.4 percent / I₂ / acetonitrile / 0.33 h / 55 °C

3: HCl / Heating

4: 81 percent / diisobutylaluminum hydride / toluene / 0.67 h / -78 °C

5: 1.) sodium acetate, sodium sulfate, acetic acid, 2.) sodium cyanoborohydride / 1.) MeOH, RT, 36 h, 2.) RT, 2 h

With hydrogenchloride; iodine; sodium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; sodium sulfate; zinc(II) chloride; In acetic acid; toluene; acetonitrile;

Reference yield:

: 5747-07-9
(Z/E)-3,5-hexadien-1-ol

: 129819-55-2
N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 3.5 h / Ambient temperature

2: potassium azide / acetonitrile; various solvent(s) / 16 h / Heating

3: 58.7 percent / LiAlH₄ / diethyl ether / 2 h / Heating

4: 1.) sodium acetate, sodium sulfate, acetic acid, 2.) sodium cyanoborohydride / 1.) MeOH, RT, 36 h, 2.) RT, 2 h

With pyridine; lithium aluminium tetrahydride; potassium azide; sodium acetate; sodium cyanoborohydride; acetic acid; sodium sulfate; In diethyl ether; acetonitrile;

Reference yield:

: 5747-08-0
1-bromo-3,5-hexadiene

: 129819-55-2
N-3,5-hexadienyl α-phenylthio-1,3-benzodioxole-5-ethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium azide / acetonitrile / 4 h / Heating

2: 58.7 percent / LiAlH₄ / diethyl ether / 2 h / Heating

3: 1.) sodium acetate, sodium sulfate, acetic acid, 2.) sodium cyanoborohydride / 1.) MeOH, RT, 36 h, 2.) RT, 2 h

With lithium aluminium tetrahydride; potassium azide; sodium acetate; sodium cyanoborohydride; acetic acid; sodium sulfate; In diethyl ether; acetonitrile;