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BEA388

Base Information
  • Chemical Name:BEA388
  • CAS No.:214139-27-2
  • Molecular Formula:C35H43N3O8
  • Molecular Weight:633.742
  • Hs Code.:
BEA<sub>388</sub>

Synonyms:

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Chemical Property of BEA388
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Technology Process of BEA388

There total 7 articles about BEA388 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1.1: Et3N / methanol / 1.17 h / 20 °C
1.2: 83 percent / pyridine / 16 h / 20 °C
2.1: 65 percent / NaOMe / methanol; CH2Cl2 / 5 h / pH 7.5
With sodium methylate; triethylamine; In methanol; dichloromethane; 1.1: Condensation / 1.2: Acetylation / 2.1: Deacetylation;
DOI:10.1139/v00-012
Guidance literature:
Multi-step reaction with 5 steps
1: 87 percent / 2-hydroxypyridine / tetrahydrofuran; CHCl3 / 0.25 h / 20 °C
2: 85 percent / camphorsulfonic acid / acetone / 0.25 h
3: N2O4; Pb(NO3)2; NaOAc / CH2Cl2 / 1.5 h / -60 - -10 °C
4: 100 percent / 30 percent aq. H2O2; LiOH / tetrahydrofuran / 0.33 h / 0 °C
With 2-hydroxypyridin; lithium hydroxide; lead(II) nitrate; camphor-10-sulfonic acid; dihydrogen peroxide; sodium acetate; dinitrogen tetraoxide; In tetrahydrofuran; dichloromethane; chloroform; acetone; 1: Ring cleavage / 2: Condensation / 3: Nitrosation / 4: Oxidation;
DOI:10.1139/v00-012
Guidance literature:
Multi-step reaction with 2 steps
1: 65 percent / NaOMe / methanol; CH2Cl2 / 5 h / pH 7.5
With sodium methylate; In methanol; dichloromethane; 1: Deacetylation;
DOI:10.1139/v00-012
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