N-Benzoylvalylphenylglycine methyl ester

Base Information

• Chemical Name: N-Benzoylvalylphenylglycine methyl ester
• CAS No.: 128992-36-9
• Molecular Formula: C₂₁H₂₄N₂O₄
• Molecular Weight: 368.433

Synonyms:

Chemical Property of N-Benzoylvalylphenylglycine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-Benzoylvalylphenylglycine methyl ester

There total 3 articles about N-Benzoylvalylphenylglycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenyl-4-isopropylidene-5(4H)oxazolone (4491-47-8) + (R)-Phenylglycine methyl ester (24461-61-8) → N-Benzoylvalylphenylglycine methyl ester (128992-37-0) + N-Benzoylvalylphenylglycine methyl ester (128992-36-9)

Guidance literature:

With hydrogen; triethylamine; palladium dichloride; In 1,2-dimethoxyethane; at 20 ℃; under 912 - 988 Torr; Rate constant; Mechanism; stereoselectivity;

DOI:10.1007/BF00960335

Reference yield:

2-phenyl-4-isopropylidene-5(4H)oxazolone (4491-47-8) → N-Benzoylvalylphenylglycine methyl ester (128992-36-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂, Et₃N / PdCl₂ / 1,2-dimethoxy-ethane / 5 h

2: Et₃N / PdCl₂ / 1,2-dimethoxy-ethane / 12 h

With hydrogen; triethylamine; palladium dichloride; In 1,2-dimethoxyethane;

DOI:10.1007/BF00960335

Reference yield:

2-phenyl-4-iso-propyl-4H-oxazolin-5-one (28897-81-6,51127-17-4,85700-33-0,5839-93-0) + (R)-Phenylglycine methyl ester (24461-61-8) → N-Benzoylvalylphenylglycine methyl ester (128992-37-0) + N-Benzoylvalylphenylglycine methyl ester (128992-36-9)

Guidance literature:

With triethylamine; palladium dichloride; In tert-butyl alcohol; for 12h; Title compound not separated from byproducts;

DOI:10.1007/BF00960335

upstream raw materials:

2-phenyl-4-isopropylidene-5(4H)oxazolone

(R)-Phenylglycine methyl ester

2-phenyl-4-iso-propyl-4H-oxazolin-5-one

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