C₂₃H₂₁FeOPS

Base Information

Chemical Name:C₂₃H₂₁FeOPS
CAS No.:74311-53-8
Molecular Formula:C₂₃H₂₁FeOPS
Molecular Weight:432.306
Hs Code.:

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Suppliers and Price of C₂₃H₂₁FeOPS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₁FeOPS

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Technology Process of C₂₃H₂₁FeOPS

There total 1 articles about C₂₃H₂₁FeOPS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 494205-48-0,173951-67-2,33056-73-4
rac-1-(diphenylphosphino)-2-(hydroxymethyl)ferrocene

: 7704-34-9
sulfur

: 497839-23-3,74311-53-8,74286-06-9
dl-1-diphenylthiophosphinyl-2-(hydroxymethyl)ferrocene

Guidance literature:: In toluene; under Ar, 100 °C for 1 h; solvent was removed in vac., column chromy. (silica, CH2Cl2:MeOH=10:1, v/v);
DOI:10.1039/b204655p

Reference yield: 98.0%

: 497839-23-3,74311-53-8,74286-06-9
dl-1-diphenylthiophosphinyl-2-(hydroxymethyl)ferrocene

: (2-(diphenylthiophosphino)ferrocenyl)methane

Guidance literature:: With borane-THF; In tetrahydrofuran; for 70h; Inert atmosphere; Reflux;
DOI:10.1039/c9dt01006h

Reference yield: 90.0%

: 74311-53-8,74286-06-9,497839-23-3
(S_p)-(2-thiodiphenylphosphino)hydroxymethylferrocene

: bis[(S_p)-(2-thiodiphenylphosphino)ferrocenylmethylene]sulfane

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; at 90 ℃; for 24h; Solvent; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejic.201700645