5'-Azido-N²-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N⁶-(4-methoxytrityl)-5',2'-dideoxyadenosine

Base Information

• Chemical Name: 5'-Azido-N²-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N⁶-(4-methoxytrityl)-5',2'-dideoxyadenosine
• CAS No.: 129789-32-8
• Molecular Formula: C₇₄H₇₃N₁₇O₁₃
• Molecular Weight: 1408.5

Synonyms:

Chemical Property of 5'-Azido-N²-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N⁶-(4-methoxytrityl)-5',2'-dideoxyadenosine

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Technology Process of 5'-Azido-N²-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N⁶-(4-methoxytrityl)-5',2'-dideoxyadenosine

There total 1 articles about 5'-Azido-N²-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N⁶-(4-methoxytrityl)-5',2'-dideoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

5'-Amino-thymidinylacetamido-<3'(O)-5'(C)>-N6-(4-methoxytrityl)-5',2'-dideoxyadenosine (129789-29-3) + Sodium; [(2R,3S,5R)-2-azidomethyl-5-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-tetrahydro-furan-3-yloxy]-acetate → 5'-Azido-N2-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N6-(4-methoxytrityl)-5',2'-dideoxyadenosine (129789-32-8)

Guidance literature:

With N-ethylmorpholine;; benzotriazol-1-ol; dicyclohexyl-carbodiimide;

DOI:10.1016/S0040-4020(01)89780-5

Reference yield: 96.0%

5'-Azido-N2-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N6-(4-methoxytrityl)-5',2'-dideoxyadenosine (129789-32-8) → 5'-Amino-N2-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N6-(4-methoxytrityl)-5',2'-dideoxyadenosine (129789-33-9)

Guidance literature:

With pyridine; ammonia; triphenylphosphine;

DOI:10.1016/S0040-4020(01)89780-5

upstream raw materials:

5'-Amino-thymidinylacetamido-<3'(O)-5'(C)>-N⁶-(4-methoxytrityl)-5',2'-dideoxyadenosine

Downstream raw materials:

5'-Amino-N²-(4-methoxytrityl)-guanosinylacetamido-<3'(O)-5'(C)>-thymidinylacetamido-<3'(O)-5'(C)>-N⁶-(4-methoxytrityl)-5',2'-dideoxyadenosine

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