Benzoic acid, 2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]- 4-fluoro-, 1-methylethyl ester

Base Information

• Chemical Name: Benzoic acid, 2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]- 4-fluoro-, 1-methylethyl ester
• CAS No.: 105756-58-9
• Molecular Formula: C15H11ClF4N2O4
• Molecular Weight: 394.71
• Mol file: 105756-58-9.mol

Synonyms:

Chemical Property of Benzoic acid, 2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]- 4-fluoro-, 1-methylethyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]- 4-fluoro-, 1-methylethyl ester

There total 1 articles about Benzoic acid, 2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]- 4-fluoro-, 1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

concentrated acetic acid + 2-chloro-4-fluoro-5-isocyanato-benzoic acid-1-methylethylester (91151-71-2) + ethyl 3-amino-4,4,4-trifluorocrotonate (141860-78-8) → isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-4-trifluoromethyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate (105756-58-9)

Guidance literature:

In N-methyl-acetamide; hexane; water;

Reference yield:

isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-4-trifluoromethyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate (105756-58-9) → isopropyl 2-chloro-5-[2-chloro-6-oxo-4-trifluoro-methyl-1(6H)-pyrimidinyl]-4-fluorobenzoate

Guidance literature:

With pyridine; In water; toluene; trichlorophosphate;

Reference yield:

isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-4-trifluoromethyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate (105756-58-9) + dimethyl sulfate (77-78-1) → 2-chloro-4-fluoro-5-(3-methyl-2,6-dioxo-4-trifluoromethyl-3,6-dihydro-2H-pyrimidin-1-yl)-benzoic acid isopropyl ester (105756-82-9)

Guidance literature:

In N-methyl-acetamide;

upstream raw materials:

2-chloro-4-fluoro-5-isocyanato-benzoic acid-1-methylethylester

ethyl 3-amino-4,4,4-trifluorocrotonate

Downstream raw materials:

2-chloro-4-fluoro-5-(3-methyl-2,6-dioxo-4-trifluoromethyl-3,6-dihydro-2H-pyrimidin-1-yl)-benzoic acid isopropyl ester

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