[phenyltris((tert-butylthio)methyl)borate]ZnBr

Base Information

Chemical Name:[phenyltris((tert-butylthio)methyl)borate]ZnBr
CAS No.:301662-97-5
Molecular Formula:C₂₁H₃₈BBrS₃Zn
Molecular Weight:542.836
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [phenyltris((tert-butylthio)methyl)borate]ZnBr

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Technology Process of [phenyltris((tert-butylthio)methyl)borate]ZnBr

There total 1 articles about [phenyltris((tert-butylthio)methyl)borate]ZnBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 213008-71-0,301663-26-3
tallium phenyltris((tert-butylthio)methyl)borate

: 7699-45-8
zinc dibromide

: 301662-97-5
[phenyltris((tert-butylthio)methyl)borate]ZnBr

Guidance literature:: In diethyl ether; dichloromethane; (PhTt(tBu))Tl in CH2Cl2 was added to ZnBr2 in Et2O, soln. was stirred for 1 h; soln. was filtered, solvent was removed under reduced pressure, residuewas washed with Et2O and recrystd. from CH2Cl2/Et2O; elem. anal.;
DOI:10.1021/ic000505q

Reference yield: 73.0%

: 301662-97-5
[phenyltris((tert-butylthio)methyl)borate]ZnBr

: 3111-52-2
potassium thiophenolate

: 301663-01-4
[phenyltris((tert-butylthio)methyl)borate]Zn(SPh)

Guidance literature:: In tetrahydrofuran; (PhTt(tBu))ZnBr in THF was added to KSPh in THF, react. for 12 h; ppt. was filtered off, solvent was removed under reduced pressure;
DOI:10.1021/ic000505q