(η5-cyclopentadienyl)(η5-C5H4SiMe3)Ti(CCC6H5)2

Base Information

Chemical Name:(η5-cyclopentadienyl)(η5-C5H4SiMe3)Ti(CCC6H5)2
CAS No.:380614-28-8
Molecular Formula:C₂₉H₂₈SiTi
Molecular Weight:452.507
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Chemical Property of (η5-cyclopentadienyl)(η5-C5H4SiMe3)Ti(CCC6H5)2

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Technology Process of (η5-cyclopentadienyl)(η5-C5H4SiMe3)Ti(CCC6H5)2

There total 1 articles about (η5-cyclopentadienyl)(η5-C5H4SiMe3)Ti(CCC6H5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 79269-70-8
dichloro(η⁵-cyclopentadienyl)[η⁵-(trimethylsilyl)cyclopentadienyl]titanium

: 536-74-3
phenylacetylene

: 380614-28-8
(η5-cyclopentadienyl)(η5-C5H4SiMe3)Ti(CCC6H5)2

Guidance literature:: With nBuLi; In tetrahydrofuran; diethyl ether; hexane; under N2; adding 2.5 M nBuLi in hexane in one portion to Et2O soln. of HCCC6H5 at -70°C, stirring for 5 min, warming to 25°C within 1 h, adding THF soln. of Ti complex in one portion, stirring at 25°C for 4 h; removal of volatiles in oil pump vac., filtration of residue in Et2O through SiO2, removal of solvents; elem. anal.;
DOI:10.1016/S0022-328X(01)01000-2