C₁₄H₁₀Cl₂N₂O₂

Base Information

• Chemical Name: C₁₄H₁₀Cl₂N₂O₂
• CAS No.: 1204524-75-3
• Molecular Formula: C₁₄H₁₀Cl₂N₂O₂
• Molecular Weight: 309.152
• Mol file: 1204524-75-3.mol

Synonyms:

Chemical Property of C₁₄H₁₀Cl₂N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₄H₁₀Cl₂N₂O₂

There total 1 articles about C₁₄H₁₀Cl₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-chloro-2-nitrobenzaldehyde (6628-86-0) + 3-chloro-p-toluidine (95-74-9,827571-80-2) → C14H10Cl2N2O2 (1204524-75-3)

Guidance literature:

In ethanol; for 2h; Reflux;

DOI:10.1021/cc9001247

Reference yield: 82.0%

bis(trichloromethyl) carbonate (32315-10-9) + C14H10Cl2N2O2 (1204524-75-3) → C30H22Cl4N4O2 (1204524-82-2)

Guidance literature:

With samarium; titanium tetrachloride; In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1021/cc9001247

Reference yield: 61.0%

C14H10Cl2N2O2 (1204524-75-3) → 5-chloro-2-(3-chloro-4-methylphenyl)-2H-indazole

Guidance literature:

With samarium; titanium tetrachloride; triethylamine; In tetrahydrofuran; for 2h; pH=8; Inert atmosphere; Reflux;

DOI:10.1002/jhet.2221

upstream raw materials:

5-chloro-2-nitrobenzaldehyde

3-chloro-p-toluidine

Downstream raw materials:

C₃₀H₂₂Cl₄N₄O₂