Technology Process of C31H43N4O3PS
There total 4 articles about C31H43N4O3PS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 18h;
Inert atmosphere;
Cooling with ice;
DOI:10.1039/c2cc32992a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: caesium carbonate / tetrahydrofuran / 20 °C / Inert atmosphere
2: tetrahydrofuran / 24 h / 20 °C / Inert atmosphere; Molecular sieve
3: sodium tetrahydroborate / tetrahydrofuran; methanol / 18 h / 20 °C / Inert atmosphere; Cooling with ice
With
sodium tetrahydroborate; caesium carbonate;
In
tetrahydrofuran; methanol;
DOI:10.1039/c2cc32992a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran / 24 h / 20 °C / Inert atmosphere; Molecular sieve
2: sodium tetrahydroborate / tetrahydrofuran; methanol / 18 h / 20 °C / Inert atmosphere; Cooling with ice
With
sodium tetrahydroborate;
In
tetrahydrofuran; methanol;
DOI:10.1039/c2cc32992a