N-(triphenylgermyl)sulfanilamide

Base Information

• Chemical Name: N-(triphenylgermyl)sulfanilamide
• CAS No.: 200729-43-7
• Molecular Formula: C₂₄H₂₂GeN₂O₂S
• Molecular Weight: 475.107
• Mol file: 200729-43-7.mol

Synonyms:

Chemical Property of N-(triphenylgermyl)sulfanilamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(triphenylgermyl)sulfanilamide

There total 1 articles about N-(triphenylgermyl)sulfanilamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

chlorotriphenylgermane (1626-24-0) + sulfanilamide (63-74-1) → N-(triphenylgermyl)sulfanilamide (200729-43-7)

Guidance literature:

With tert.-butyl lithium; In tetrahydrofuran; pentane; byproducts: LiCl; double vac. ramp, N2 or Ar; sulfamide soln. addn. dropwise to Li-compd. soln. (pentane) at -78°C, mixt. warming to ambient temp. over 30 min (stirring), Ge-compd. soln. (THF) addn., stirring (20°C, 4 h), THF replacing by C6H6, LiCl removal; soln. concn. (1E-2 mm Hg), recrystn. (pentane, -30°C, 17 h);

DOI:10.1080/10426509608038772

upstream raw materials:

chlorotriphenylgermane

sulfanilamide