3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium tetrafluoroborate

Base Information

• Chemical Name: 3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium tetrafluoroborate
• CAS No.: 1272971-16-0
• Molecular Formula: BF₄*C₁₈H₁₉N₂O
• Molecular Weight: 366.166
• Mol file: 1272971-16-0.mol

Synonyms:

Chemical Property of 3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium tetrafluoroborate

Chemical Property:

Purity/Quality:

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Technology Process of 3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium tetrafluoroborate

There total 1 articles about 3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium chloride (1272971-13-7) → 3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium tetrafluoroborate (1272971-16-0)

Guidance literature:

With silver tetrafluoroborate; In acetone; for 12h; Darkness;

DOI:10.1021/om101173e

Reference yield: 61.0%

Os(hydride)6(triisopropylphosphine)2 (131296-74-7) + 3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium tetrafluoroborate (1272971-16-0) → [OsH3(P(iso-propyl)3)2(3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium(-3H))] tetrafluoroborate

Guidance literature:

In tetrahydrofuran; under rigorous exclusion of air using Schlenk techniques; soln. of Os complex in THF was treated with 1.2 equiv. of imidazolium salt; soln. heated under reflux for 29 h; cooled to room temp.; filtered; solvent removed (vac.); Et2O added; solid washed (Et2O); dried(vac.); elem. anal.;

DOI:10.1021/om101173e

upstream raw materials:

3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium chloride