{2,3-diberezyl-4-acetyl L-fucose}-alpha-1-4-[2',3'-dibenzyl 6'-acetyl-glucose]-beta-1-2(3,4 dibenzyl alpha methyl L-fucose)

Base Information

Chemical Name:{2,3-diberezyl-4-acetyl L-fucose}-alpha-1-4-[2',3'-dibenzyl 6'-acetyl-glucose]-beta-1-2(3,4 dibenzyl alpha methyl L-fucose)
CAS No.:1415117-96-2
Molecular Formula:C₆₅H₇₄O₁₆
Molecular Weight:1111.29
Hs Code.:

Synonyms:

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Chemical Property of {2,3-diberezyl-4-acetyl L-fucose}-alpha-1-4-[2',3'-dibenzyl 6'-acetyl-glucose]-beta-1-2(3,4 dibenzyl alpha methyl L-fucose)

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Technology Process of {2,3-diberezyl-4-acetyl L-fucose}-alpha-1-4-[2',3'-dibenzyl 6'-acetyl-glucose]-beta-1-2(3,4 dibenzyl alpha methyl L-fucose)

There total 2 articles about {2,3-diberezyl-4-acetyl L-fucose}-alpha-1-4-[2',3'-dibenzyl 6'-acetyl-glucose]-beta-1-2(3,4 dibenzyl alpha methyl L-fucose) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42822-13-9
methyl 3,4-di-O-benzyl-α-L-fucopyranoside

: 1415117-96-2
{2,3-diberezyl-4-acetyl L-fucose}-alpha-1-4-[2',3'-dibenzyl 6'-acetyl-glucose]-beta-1-2(3,4 dibenzyl alpha methyl L-fucose)

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide / dichloromethane / 20 °C / 4A molecular sieve

1.2: 0.5 h

2.1: sodium methylate; methanol / 4 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h

3.2: 1 h

4.1: 1,2-dichloro-ethane / 24 h / 70 °C

5.1: dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate / dichloromethane / 2 h / 20 °C / 4A molecular sieve

With methanol; N-iodo-succinimide; sodium methylate; sodium hydride; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 4',6'-benzylidene-2,3 dibenzoyl-1-thiomethyl D-glucose

: 1415117-96-2
{2,3-diberezyl-4-acetyl L-fucose}-alpha-1-4-[2',3'-dibenzyl 6'-acetyl-glucose]-beta-1-2(3,4 dibenzyl alpha methyl L-fucose)

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide / dichloromethane / 20 °C / 4A molecular sieve

1.2: 0.5 h

2.1: sodium methylate; methanol / 4 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h

3.2: 1 h

4.1: 1,2-dichloro-ethane / 24 h / 70 °C

5.1: dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate / dichloromethane / 2 h / 20 °C / 4A molecular sieve

With methanol; N-iodo-succinimide; sodium methylate; sodium hydride; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;