[(benzyl)3tin(IV)(furfuraldehyde thiosemicarbazone(-H))]

Base Information

Chemical Name:[(benzyl)3tin(IV)(furfuraldehyde thiosemicarbazone(-H))]
CAS No.:1290545-09-3
Molecular Formula:C₂₇H₂₇N₃OSSn
Molecular Weight:560.307
Hs Code.:

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Chemical Property of [(benzyl)3tin(IV)(furfuraldehyde thiosemicarbazone(-H))]

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Technology Process of [(benzyl)3tin(IV)(furfuraldehyde thiosemicarbazone(-H))]

There total 1 articles about [(benzyl)3tin(IV)(furfuraldehyde thiosemicarbazone(-H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.1%

: 5419-96-5,153750-93-7
furan-2-aldehyde thiosemicarbazone

: 3151-41-5
tribenzyltin(IV) chloride

: 1290545-09-3
[(benzyl)3tin(IV)(furfuraldehyde thiosemicarbazone(-H))]

Guidance literature:: With NaH; isopropanol; In tetrahydrofuran; isopropyl alcohol; byproducts: NaCl; soln. of NaH in isopropanol stirred for 0.5 h, soln. of the thiosemicarbazone in THF added dropwise, mixt. refluxed for 2 h, cooled to room temp., Bz3SnCl added dropwise, refluxed for 24 h, cooled to room temp.; soln. filtered, filtrate evapd. under vac., residue washed with hexane and cyclohexane, dried under vac. for 1 h; elem. anal.;
DOI:10.1080/15533174.2010.522674