Technology Process of C17H24O3
There total 2 articles about C17H24O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dodecacarbonyl-triangulo-triruthenium; carbon monoxide; tetrabutyl-ammonium chloride; water; triethylamine;
In
1,4-dioxane;
at 75 ℃;
for 24h;
under 2068.65 Torr;
Overall yield = 73 %; Overall yield = 203 mg; chemoselective reaction;
Glovebox;
Autoclave;
DOI:10.1021/jo501004j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 1.17 h / 0 - 23 °C / Inert atmosphere; Autoclave
2: dodecacarbonyl-triangulo-triruthenium; carbon monoxide; tetrabutyl-ammonium chloride; triethylamine; water / 1,4-dioxane / 24 h / 75 °C / 2068.65 Torr / Glovebox; Autoclave
With
pyridine; dodecacarbonyl-triangulo-triruthenium; carbon monoxide; tetrabutyl-ammonium chloride; water; triethylamine;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/jo501004j