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Benzene, 1-[(2-chloro-2-phenylethyl)sulfonyl]-4-methoxy-, (S)-

Base Information Edit
  • Chemical Name:Benzene, 1-[(2-chloro-2-phenylethyl)sulfonyl]-4-methoxy-, (S)-
  • CAS No.:105769-53-7
  • Molecular Formula:C15H15ClO3S
  • Molecular Weight:310.801
  • Hs Code.:
  • Mol file:105769-53-7.mol
Benzene, 1-[(2-chloro-2-phenylethyl)sulfonyl]-4-methoxy-, (S)-

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of Benzene, 1-[(2-chloro-2-phenylethyl)sulfonyl]-4-methoxy-, (S)- Edit
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Technology Process of Benzene, 1-[(2-chloro-2-phenylethyl)sulfonyl]-4-methoxy-, (S)-

There total 8 articles about Benzene, 1-[(2-chloro-2-phenylethyl)sulfonyl]-4-methoxy-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With thionyl chloride; In chloroform; for 3h; Heating;
DOI:10.1021/jo00391a025
Guidance literature:
Multi-step reaction with 8 steps
1: p-toluenesulfonic acid monohydrate / CH2Cl2 / 24 h / Heating
2: p-toluenesulfonic acid monohydrate / CH2Cl2 / 2 h / 20 °C
3: LiAlH4 / diethyl ether / 2 h / Heating
4: pyridine / 24 h / 0 - 5 °C
5: methanol; dimethylformamide / 12 h / 100 °C
6: CH3COOH, H2O / tetrahydrofuran / 12 h / 45 °C
7: m-chloroperbenzoic acid / CH2Cl2 / 24 h / Ambient temperature
8: SOCl2 / CHCl3 / 3 h / Heating
With lithium aluminium tetrahydride; thionyl chloride; water; toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00391a025
Guidance literature:
Multi-step reaction with 7 steps
1: p-toluenesulfonic acid monohydrate / CH2Cl2 / 2 h / 20 °C
2: LiAlH4 / diethyl ether / 2 h / Heating
3: pyridine / 24 h / 0 - 5 °C
4: methanol; dimethylformamide / 12 h / 100 °C
5: CH3COOH, H2O / tetrahydrofuran / 12 h / 45 °C
6: m-chloroperbenzoic acid / CH2Cl2 / 24 h / Ambient temperature
7: SOCl2 / CHCl3 / 3 h / Heating
With lithium aluminium tetrahydride; thionyl chloride; water; toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00391a025
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