Technology Process of C17H25NO4
There total 3 articles about C17H25NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium chloride; lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere
2.1: dichloromethane / 2 h / Inert atmosphere
3.1: sodium hydroxide / 1,4-dioxane; water / pH 12 / Inert atmosphere
3.2: Inert atmosphere
3.3: Inert atmosphere
With
lithium chloride; sodium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1039/c0ob00890g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dichloromethane / 2 h / Inert atmosphere
2.1: sodium hydroxide / 1,4-dioxane; water / pH 12 / Inert atmosphere
2.2: Inert atmosphere
2.3: Inert atmosphere
With
sodium hydroxide;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1039/c0ob00890g
- Guidance literature:
-
C2HF3O2*C12H17NO2;
With
sodium hydroxide;
In
1,4-dioxane; water;
pH=12;
Inert atmosphere;
di-tert-butyl dicarbonate;
In
1,4-dioxane; water;
Inert atmosphere;
With
hydrogenchloride;
In
1,4-dioxane; water;
Inert atmosphere;
DOI:10.1039/c0ob00890g