Technology Process of C26H39ClN4O8SSi
There total 11 articles about C26H39ClN4O8SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
morpholine; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
at 0 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/jm1014023
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere
2: morpholine; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
With
morpholine; tetrakis(triphenylphosphine) palladium(0); toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol;
DOI:10.1021/jm1014023
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triethylamine / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere
2.1: chloro-trimethyl-silane; sodium iodide / acetonitrile / 0.08 h / 20 °C / Inert atmosphere
2.2: 2.08 h / 0 - 20 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere
4.1: trifluoroacetic acid / 0.5 h / 0 °C / Inert atmosphere
5.1: 1,2-dichloro-ethane / acetonitrile / 5 h / 0 °C / Inert atmosphere
6.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere
7.1: morpholine; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
With
morpholine; tetrakis(triphenylphosphine) palladium(0); chloro-trimethyl-silane; toluene-4-sulfonic acid; 1,2-dichloro-ethane; triethylamine; trifluoroacetic acid; sodium iodide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm1014023
