C₁₉H₁₉IO

Base Information

Chemical Name:C₁₉H₁₉IO
CAS No.:1289154-80-8
Molecular Formula:C₁₉H₁₉IO
Molecular Weight:390.264
Hs Code.:

Synonyms:

Suppliers and Price of C₁₉H₁₉IO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₁₉IO

Chemical Property:

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Technology Process of C₁₉H₁₉IO

There total 1 articles about C₁₉H₁₉IO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 938-16-9
2,2-dimethylpropiophenone

: 766-50-7
(2-iodophenyl)-acetylene

: 1289154-80-8
C₁₉H₁₉IO

Guidance literature:: (2-iodophenyl)-acetylene; With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

2,2-dimethylpropiophenone; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.3762/bjoc.7.58

Reference yield:

: 1289154-80-8
C₁₉H₁₉IO

: 1289154-86-4
C₂₄H₂₈Si

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane; trifluoroacetic acid

2: copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; triethylamine / toluene / 5 h / 70 °C

With triethylsilane; copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; triethylamine; trifluoroacetic acid; In toluene; 2: Sonogashira reaction;
DOI:10.3762/bjoc.7.58

Reference yield:

: 1289154-80-8
C₁₉H₁₉IO

: 1289154-87-5
C₂₁H₂₀

Guidance literature:: Multi-step reaction with 3 steps

1: triethylsilane; trifluoroacetic acid

2: copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; triethylamine / toluene / 5 h / 70 °C

3: water; sodium hydroxide / methanol; diethyl ether / 0.5 h / 20 °C

With triethylsilane; copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; water; triethylamine; trifluoroacetic acid; sodium hydroxide; In methanol; diethyl ether; toluene; 2: Sonogashira reaction;
DOI:10.3762/bjoc.7.58