3-ethyl 5-methyl 2-[(2-{[(diethoxyphosphoryl)(2-thienyl)methyl]amino}ethoxy)methyl]-4-(2-chlorophenyl)-6-methyl-1,4-dihydro-3,5-pyridenedicarboxylate

Base Information

Chemical Name:3-ethyl 5-methyl 2-[(2-{[(diethoxyphosphoryl)(2-thienyl)methyl]amino}ethoxy)methyl]-4-(2-chlorophenyl)-6-methyl-1,4-dihydro-3,5-pyridenedicarboxylate
CAS No.:1376703-05-7
Molecular Formula:C₂₉H₃₈ClN₂O₈PS
Molecular Weight:641.122
Hs Code.:

3-ethyl 5-methyl 2-[(2-{[(diethoxyphosphoryl)(2-thienyl)methyl]amino}ethoxy)methyl]-4-(2-chlorophenyl)-6-methyl-1,4-dihydro-3,5-pyridenedicarboxylate

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Chemical Property of 3-ethyl 5-methyl 2-[(2-{[(diethoxyphosphoryl)(2-thienyl)methyl]amino}ethoxy)methyl]-4-(2-chlorophenyl)-6-methyl-1,4-dihydro-3,5-pyridenedicarboxylate

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Technology Process of 3-ethyl 5-methyl 2-[(2-{[(diethoxyphosphoryl)(2-thienyl)methyl]amino}ethoxy)methyl]-4-(2-chlorophenyl)-6-methyl-1,4-dihydro-3,5-pyridenedicarboxylate

There total 1 articles about 3-ethyl 5-methyl 2-[(2-{[(diethoxyphosphoryl)(2-thienyl)methyl]amino}ethoxy)methyl]-4-(2-chlorophenyl)-6-methyl-1,4-dihydro-3,5-pyridenedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88150-42-9
2-[(2-aminoethoxy)methyl]-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

: 1376703-05-7
3-ethyl 5-methyl 2-[(2-{[(diethoxyphosphoryl)(2-thienyl)methyl]amino}ethoxy)methyl]-4-(2-chlorophenyl)-6-methyl-1,4-dihydro-3,5-pyridenedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 0.17 h / Molecular sieve; Sonication; Reflux

2: tin(II) chloride dihdyrate / 0.33 h / 75 °C / Sonication

With tin(II) chloride dihdyrate; In ethanol; 2: Pudovik reaction;
DOI:10.1002/ardp.201100256