meso-2-fluorenyl-1,2-diphenylethanol

Base Information

Chemical Name:meso-2-fluorenyl-1,2-diphenylethanol
CAS No.:139219-54-8
Molecular Formula:C₂₇H₂₂O
Molecular Weight:362.471
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-2-fluorenyl-1,2-diphenylethanol

Chemical Property:

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Technology Process of meso-2-fluorenyl-1,2-diphenylethanol

There total 2 articles about meso-2-fluorenyl-1,2-diphenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86-73-7
9H-fluorene

: 1439-07-2
trans-Stilbene oxide

: 139219-53-7,139219-54-8
2-fluorenyl(1,2-diphenyl)ethanol

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, diethyl ether, 0 deg C, 2.) hexane, diethyl ether, 0 deg C, overnight;
DOI:10.1016/0022-328X(91)86470-B

Reference yield:

: 86-73-7
9H-fluorene

: 1689-71-0
cis-1,2-diphenyloxirane

: 139219-53-7,139219-54-8
meso-2-fluorenyl-1,2-diphenylethanol

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, diethyl ether, 0 deg C, 2.) hexane, diethyl ether, 0 deg C, overnight;
DOI:10.1016/0022-328X(91)86470-B

Reference yield:

: 21959-01-3,125410-70-0,125410-71-1
zirconium tetrachloride bis(tetrahydrofuran) complex

: 139219-53-7,139219-54-8
meso-2-fluorenyl-1,2-diphenylethanol

: (meso-2-(η5-fluorenyl)(diphenylethoxy))ZrCl2(thf)2

Guidance literature:: With n-butyllithium; In tetrahydrofuran; 2 equivalents of BuLi (in hexane) was added to a soln. of alcohol at 0 ° C, addn. of ZrCl4(thf)2 at -70 ° C, soln. refluxed for ca. 4 h; evapn., suspn. of the residual powder in CH2Cl2 filtered through celite, evapn., extn. with boiling heptane,;
DOI:10.1016/0022-328X(91)86470-B