5-N,6-S-(N'-phenyliminomethylidene)-1-deoxy-6-thiogalactonojirimycin

Base Information

• Chemical Name: 5-N,6-S-(N'-phenyliminomethylidene)-1-deoxy-6-thiogalactonojirimycin
• CAS No.: 1383691-30-2
• Molecular Formula: C₁₃H₁₆N₂O₃S
• Molecular Weight: 280.348
• Mol file: 1383691-30-2.mol

Synonyms:

Chemical Property of 5-N,6-S-(N'-phenyliminomethylidene)-1-deoxy-6-thiogalactonojirimycin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-N,6-S-(N'-phenyliminomethylidene)-1-deoxy-6-thiogalactonojirimycin

There total 2 articles about 5-N,6-S-(N'-phenyliminomethylidene)-1-deoxy-6-thiogalactonojirimycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(N'-phenylthiocarbamoyl)-1-deoxygalactonojirimycin → 5-N,6-S-(N'-phenyliminomethylidene)-1-deoxy-6-thiogalactonojirimycin (1383691-30-2)

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃; for 12h; pH=1;

DOI:10.1039/c2cc32065g

Reference yield:

1-deoxygalactonojirimycin (108147-54-2) + phenyl isothiocyanate (103-72-0) → 5-N,6-S-(N'-phenyliminomethylidene)-1-deoxy-6-thiogalactonojirimycin (1383691-30-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; triethylamine / 18 h / 20 °C

2: hydrogenchloride / methanol / 12 h / 20 °C / pH 1

With pyridine; hydrogenchloride; triethylamine; In methanol;

DOI:10.1039/c2cc32065g

upstream raw materials:

1-deoxygalactonojirimycin

phenyl isothiocyanate