Technology Process of C39H40N2O3
There total 4 articles about C39H40N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: iodine / 0.5 h / 20 °C / Inert atmosphere
2: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; caesium carbonate / toluene / 20 h / 80 °C / Inert atmosphere
3: water; sodium hydroxide / tetrahydrofuran / 20 h / Reflux
With
1,1'-bis-(diphenylphosphino)ferrocene; water; iodine; palladium diacetate; caesium carbonate; sodium hydroxide;
In
tetrahydrofuran; toluene;
2: Hartwig-Buchwald cross coupling;
DOI:10.1002/chem.201103411
- Guidance literature:
-
With
water; sodium hydroxide;
In
tetrahydrofuran;
for 20h;
Reflux;
DOI:10.1002/chem.201103411
- Guidance literature:
-
Multi-step reaction with 4 steps
1: borane-THF / tetrahydrofuran / 72 h / 20 °C / Inert atmosphere
2: iodine / 0.5 h / 20 °C / Inert atmosphere
3: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; caesium carbonate / toluene / 20 h / 80 °C / Inert atmosphere
4: water; sodium hydroxide / tetrahydrofuran / 20 h / Reflux
With
1,1'-bis-(diphenylphosphino)ferrocene; borane-THF; water; iodine; palladium diacetate; caesium carbonate; sodium hydroxide;
In
tetrahydrofuran; toluene;
3: Hartwig-Buchwald cross coupling;
DOI:10.1002/chem.201103411
