Technology Process of C61H98N6O16
There total 13 articles about C61H98N6O16 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 2 h / 20 °C
2: acetic acid / dichloromethane / 0.5 h / 20 °C
3: sodium tris(acetoxy)borohydride / 1.5 h / 20 °C
With
sulfur trioxide pyridine complex; sodium tris(acetoxy)borohydride; acetic acid; triethylamine;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm200906r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid / dichloromethane / 0.5 h / 20 °C
2: sodium tris(acetoxy)borohydride / 1.5 h / 20 °C
With
sodium tris(acetoxy)borohydride; acetic acid;
In
dichloromethane;
DOI:10.1021/jm200906r
- Guidance literature:
-
Multi-step reaction with 7 steps
1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 92 h / 40 °C
2: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 20 °C
3: hydrogenchloride / ethyl acetate / 3 h / 20 °C
4: sodium hydrogencarbonate / water; ethyl acetate / 8 h / 0 °C
5: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 2 h / 20 °C
6: acetic acid / dichloromethane / 0.5 h / 20 °C
7: sodium tris(acetoxy)borohydride / 1.5 h / 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; palladium 10% on activated carbon; hydrogen; sulfur trioxide pyridine complex; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; acetic acid; triethylamine;
In
methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm200906r