4-Methyl-3-pentadecyl-veratrol

Base Information

• Chemical Name: 4-Methyl-3-pentadecyl-veratrol
• CAS No.: 16273-17-9
• Molecular Formula: C₂₄H₄₂O₂
• Molecular Weight: 362.596
• Mol file: 16273-17-9.mol

Synonyms:

Chemical Property of 4-Methyl-3-pentadecyl-veratrol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Methyl-3-pentadecyl-veratrol

There total 1 articles about 4-Methyl-3-pentadecyl-veratrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentadecyl bromide (629-72-1) + 1,2-dimethoxy-4-methylbenzene (494-99-5) → 5-Methyl-3-pentadecyl-veratrol (16273-09-9) + 4-Methyl-3-pentadecyl-veratrol (16273-17-9)

Guidance literature:

With n-butyllithium; Multistep reaction; 1.) THF, hexane, a) 0 deg C, 2.5 h, b) reflux, 0.5 h, 2.) THF, hexane, a) RT, 0.5 h, b) reflux, 17 h;

DOI:10.1021/jm00133a007

Reference yield:

4-Methyl-3-pentadecyl-veratrol (16273-17-9) → 4-Methyl-3-pentadecyl-brenzcatechin (16273-11-3)

Guidance literature:

With boron tribromide; In dichloromethane; for 1h;

DOI:10.1021/jm00133a007

Reference yield:

4-Methyl-3-pentadecyl-veratrol (16273-17-9) → 4-Methyl-3-pentadecyl-[1,2]benzoquinone (22693-11-4)

Guidance literature:

Multi-step reaction with 2 steps

1: BBr₃ / CH₂Cl₂ / 1 h

2: Ag₂O, Na₂SO₄ / diethyl ether / 0.07 h

With boron tribromide; sodium sulfate; silver(l) oxide; In diethyl ether; dichloromethane;

DOI:10.1021/jm00133a007

upstream raw materials:

pentadecyl bromide

1,2-dimethoxy-4-methylbenzene

Downstream raw materials:

4-Methyl-3-pentadecyl-brenzcatechin

4-Methyl-3-pentadecyl-[1,2]benzoquinone