C₃₄H₂₆Cl₂N₂O₆

Base Information

• Chemical Name: C₃₄H₂₆Cl₂N₂O₆
• CAS No.: 1453486-13-9
• Molecular Formula: C₃₄H₂₆Cl₂N₂O₆
• Molecular Weight: 629.496
• Mol file: 1453486-13-9.mol

Synonyms:

Chemical Property of C₃₄H₂₆Cl₂N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₆Cl₂N₂O₆

There total 1 articles about C₃₄H₂₆Cl₂N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 3,3'-bis(4-chlorophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-biindole → C34H26Cl2N2O6 (1453486-13-9)

Guidance literature:

N,N-dimethyl-formamide; 3,3'-bis(4-chlorophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-biindole; With trichlorophosphate; at 20 - 60 ℃; for 8.5h;

With water; sodium hydroxide; at 20 ℃; for 1h;

DOI:10.1055/s-0033-1338868

Reference yield:

C34H26Cl2N2O6 (1453486-13-9) → C34H30Cl2N2O6 (1453486-16-2)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 20 ℃; for 8h;

DOI:10.1055/s-0033-1338868

Reference yield:

C34H26Cl2N2O6 (1453486-13-9) → C68H54Cl4N4O10 (1453486-19-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 8 h / 20 °C

2: toluene-4-sulfonic acid / isopropyl alcohol / 32 h

With sodium tetrahydroborate; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; isopropyl alcohol;

DOI:10.1055/s-0033-1338868

upstream raw materials:

N,N-dimethyl-formamide

Downstream raw materials:

C₆₈H₅₄Cl₄N₄O₁₀

C₅₈H₅₂Cl₂N₄O₁₀

C₆₈H₅₈Cl₄N₄O₁₀

C₅₈H₅₆Cl₂N₄O₁₀