4-acetamidophenyl phenyl selenide

Base Information

• Chemical Name: 4-acetamidophenyl phenyl selenide
• CAS No.: 861062-67-1
• Molecular Formula: C₁₄H₁₃NOSe
• Molecular Weight: 290.223
• Mol file: 861062-67-1.mol

Synonyms:

Chemical Property of 4-acetamidophenyl phenyl selenide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-acetamidophenyl phenyl selenide

There total 8 articles about 4-acetamidophenyl phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

benzeneselenenyl m-nitrobenzenesulfonate (133708-80-2) + Acetanilid (103-84-4) → 4-acetamidophenyl phenyl selenide (861062-67-1)

Guidance literature:

In dichloromethane; 1) r.t., 1 h, 2) 2 h, reflux;

DOI:10.1246/bcsj.64.416

Reference yield:

Acetanilid (103-84-4) → 4-acetamidophenyl phenyl selenide (861062-67-1)

Guidance literature:

With Phenylselenyl chloride; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4039(00)81848-1

Reference yield:

diphenyl diselenide (1666-13-3) → 4-acetamidophenyl phenyl selenide (861062-67-1)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 0.17 h / 0 °C

2: 84 percent / CH₂Cl₂ / 1) r.t., 1 h, 2) 2 h, reflux

In dichloromethane; acetonitrile;

DOI:10.1246/bcsj.64.416

upstream raw materials:

4-aminophenyl phenyl selenide

acetic anhydride

benzeneselenenyl m-nitrobenzenesulfonate

Acetanilid

Downstream raw materials:

4-aminophenyl phenyl selenide

4-benzeneseleninyl-aniline