N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

Base Information

Chemical Name:N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester
CAS No.:161959-13-3
Molecular Formula:C₃₁H₂₈N₄O₂S₄
Molecular Weight:616.853
Hs Code.:

N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

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Chemical Property of N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

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Technology Process of N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

There total 1 articles about N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.7%

: 13331-31-2
S-benzyldithiocarbazate

: 3046-82-0
5,5'-methylenebis(salicylaldehyde)

: 161959-13-3
N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

Guidance literature:: In methanol; for 3h; Reflux;
DOI:10.1002/ejic.201200012

Reference yield: 80.5%

: 3153-26-2
bis(acetylacetonate)oxovanadium

: 161959-13-3
N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

: [CH₂(V(O)(H₂O)(OC₆H₃CHNNC(S)(SCH₂C₆H₅)))2]

Guidance literature:: In methanol; V complex soln. (10 mmol) added to soln. of CH2(C6H3(OH)(CHNNHC(S)(SCH2C6H5)))2 (5 mmol) with shaking, heated at reflux for 4 h; concd., kept at room temp. for 10 h, ppt. filtered off, washed with MeOH, dried (under silica gel); elem. anal.;
DOI:10.1002/ejic.201200012

Reference yield: 72.8%

: 3153-26-2
bis(acetylacetonate)oxovanadium

: cesiumhydroxide monohydrate

: 161959-13-3
N'-[1-{5-[3-(Benzylsulfanylthiocarbonyl-hydrazonomethyl)-4-hydroxy-benzyl]-2-hydroxy-phenyl}-meth-(E)-ylidene]-hydrazinecarbodithioic acid benzyl ester

: 2Cs⁽¹⁺⁾*[CH₂(V(O)2(OC₆H₃CHNNC(S)(SCH₂C₆H₅)))2]^(2-)*2H₂O=Cs₂[CH₂(VO₂(OC₆H₃CHNNC(S)(SCH₂C₆H₅)))2]*2H₂O

Guidance literature:: With air; In methanol; soln. of V complex (2 mmol) added to soln. of CH2(C6H3(OH)(CHNNHC(S)SCH2C6H5))2 (1 mmol) at stirring, heated at reflux for 4 h, CsOH*H2O added (2.4 mmol), heated at reflux for 2 h, oxidized in air; slow evapd. at room temp. for 2 d, kept at room temp. overnight, ppt. filtered off, washed with MeOH, dried under silica gel; elem. anal.;
DOI:10.1002/ejic.201200012