Technology Process of 1,1,5,5-Tetraphenyl-pentan-3-aldehyde
There total 8 articles about 1,1,5,5-Tetraphenyl-pentan-3-aldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 1h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 70 percent / Mn(OAc)3*2H2O, gl. AcOH / 1 h / Heating
2: 78 percent / NaOH / ethanol / 1 h / Heating
3: 75 percent / PBr3 / toluene / 1 h / Ambient temperature
4: 50 percent / NaBH4 / methanol / 1 h
5: H2 / 10percent Pd/C / methanol / 12 h / 1838.8 Torr
6: 70 percent / pyridinium chlorochromate / CH2Cl2 / 1 h
With
sodium hydroxide; sodium tetrahydroborate; hydrogen; manganese triacetate; phosphorus tribromide; acetic acid; pyridinium chlorochromate;
palladium on activated charcoal;
In
methanol; ethanol; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 78 percent / NaOH / ethanol / 1 h / Heating
2: 75 percent / PBr3 / toluene / 1 h / Ambient temperature
3: 50 percent / NaBH4 / methanol / 1 h
4: H2 / 10percent Pd/C / methanol / 12 h / 1838.8 Torr
5: 70 percent / pyridinium chlorochromate / CH2Cl2 / 1 h
With
sodium hydroxide; sodium tetrahydroborate; hydrogen; phosphorus tribromide; pyridinium chlorochromate;
palladium on activated charcoal;
In
methanol; ethanol; dichloromethane; toluene;