C₂₂H₃₆O₄Si

Base Information

Chemical Name:C₂₂H₃₆O₄Si
CAS No.:1355616-33-9
Molecular Formula:C₂₂H₃₆O₄Si
Molecular Weight:392.611
Hs Code.:

C<sub>22</sub>H<sub>36</sub>O<sub>4</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₆O₄Si

Chemical Property:

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Technology Process of C₂₂H₃₆O₄Si

There total 4 articles about C₂₂H₃₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₆O₄Si

: C₂₂H₃₆O₄Si

: 1355616-33-9
C₂₂H₃₆O₄Si

Guidance literature:: C₂₂H₃₆O₄Si; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - -45 ℃; for 2h; Inert atmosphere;

With triphenylacetic acid; In tetrahydrofuran; hexane; at -78 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ml200254h

Reference yield:

: 1254369-08-8
C₁₆H₂₂O₃

: C₂₂H₃₆O₄Si

: 1355616-33-9
C₂₂H₃₆O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium osmate; K₃Fe(CN)6; (DHQD)2PHAL; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 36 h / 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 - -45 °C / Inert atmosphere

4.2: 2 h / -78 °C / Inert atmosphere

With 1H-imidazole; potassium osmate; methanesulfonamide; K₃Fe(CN)6; (DHQD)2PHAL; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; hexane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Sharpless dihydroxylation;
DOI:10.1021/ml200254h

Reference yield:

: 1355616-31-7
C₁₅H₂₀O₄

: C₂₂H₃₆O₄Si

: 1355616-33-9
C₂₂H₃₆O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 - -45 °C / Inert atmosphere

3.2: 2 h / -78 °C / Inert atmosphere

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/ml200254h