RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

Base Information

Chemical Name:RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)
CAS No.:138980-90-2
Molecular Formula:C₂₆H₂₆Cl₂N₅PRu
Molecular Weight:611.476
Hs Code.:

RuCl<sub>2</sub>(P(CH<sub>3</sub>)3)(C<sub>5</sub>H<sub>3</sub>N(C<sub>3</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)N<sub>2</sub>)2)

Synonyms:

Suppliers and Price of RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

Chemical Property:

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Technology Process of RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

There total 1 articles about RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 139779-41-2
RuCl₃(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

: 594-09-2
trimethylphosphane

: 138980-90-2,139894-97-6
RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

Guidance literature:: With triethylamine; In dichloromethane; addn. of 1.5 equivalents of P(CH3)3 and triethylamine to a suspension of the Ru(III) complex in CH2Cl2; refluxing for 10-24 h; performed under N2;; the ppt. was vac. filtered, washed with abs. ethanol and diethyl ether and purified, if necessary, by chromy. (basic Al2O3, 2% CH3OH/CH2Cl2); evapn.; dissolving in CH2Cl2 and dropwise addn. into hexanes;;
DOI:10.1039/DT9930001563

Reference yield:

: 138980-90-2,139894-97-6
RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

: 139894-97-6
RuCl₂(P(CH₃)3)(C₅H₃N(C₃H₂(C₆H₅)N₂)2)

Guidance literature:: In 1,2-dichloro-ethane; Irradiation (UV/VIS); irradiation of the trans complex in 1,2-dichloroethane for 48-61 h with a 120 W tungsten light; performed under N2;; filtration; the filtrate was evapd. to dryness; the ppt. was slurried in CH2Cl2 and titurated into hexanes or (C2H5)2O; vac. filtration;;
DOI:10.1039/DT9930001563