Technology Process of C25H23N3O4S
There total 8 articles about C25H23N3O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: sodium tetrahydroborate / methanol
2: 1H-imidazole
3: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)
4: n-butyllithium / tetrahydrofuran
5: dicyclohexyl-carbodiimide
6: Burgess Reagent; triethylamine / acetonitrile / 80 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran
8: thionyl chloride / toluene
9: N-ethyl-N,N-diisopropylamine / acetonitrile
10: water; sodium hydroxide / ethanol
With
1H-imidazole; sodium tetrahydroborate; n-butyllithium; thionyl chloride; Burgess Reagent; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); tetrabutyl ammonium fluoride; water; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / toluene
2: N-ethyl-N,N-diisopropylamine / acetonitrile
3: water; sodium hydroxide / ethanol
With
thionyl chloride; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
ethanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / acetonitrile
2: water; sodium hydroxide / ethanol
With
water; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
ethanol; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
