[(μ2-1,2,4,5-tetracarboxylic acid(2-))0.5 (μ4-1,2,4,5-tetracarboxylic acid(2-))0.5 zinc(II) (1,10-phenanthroline) (water)]n

Base Information

Chemical Name:[(μ2-1,2,4,5-tetracarboxylic acid(2-))0.5 (μ4-1,2,4,5-tetracarboxylic acid(2-))0.5 zinc(II) (1,10-phenanthroline) (water)]n
CAS No.:1000598-43-5
Molecular Formula:C₁₀H₄O₈*C₁₂H₈N₂*H₂O*Zn
Molecular Weight:515.751
Hs Code.:

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Chemical Property of [(μ2-1,2,4,5-tetracarboxylic acid(2-))0.5 (μ4-1,2,4,5-tetracarboxylic acid(2-))0.5 zinc(II) (1,10-phenanthroline) (water)]n

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Technology Process of [(μ2-1,2,4,5-tetracarboxylic acid(2-))0.5 (μ4-1,2,4,5-tetracarboxylic acid(2-))0.5 zinc(II) (1,10-phenanthroline) (water)]n

There total 1 articles about [(μ2-1,2,4,5-tetracarboxylic acid(2-))0.5 (μ4-1,2,4,5-tetracarboxylic acid(2-))0.5 zinc(II) (1,10-phenanthroline) (water)]n which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 66-71-7
1,10-Phenanthroline

: 89-05-4
1,2,4,5-benzenetetracarboxylic acid

: 7732-18-5
water

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1000598-43-5
[(μ2-1,2,4,5-tetracarboxylic acid(2-))0.5 (μ4-1,2,4,5-tetracarboxylic acid(2-))0.5 zinc(II) (1,10-phenanthroline) (water)]n

Guidance literature:: With NaOH; In water; High Pressure; ZnCl2, benzene-1,2,4,5-tetracarboxylic acid, 1,10-phenanthroline and H2Ostirred for 2 h in air at room temp.; pH adjusted to 3.0 with aq. NaOH; resulting solid sealed and heated in steel autoclave at 170 °C f or 4 h under autogenous pressure; after slowly cooling to ambient temp.; the obtained crystals washed withdistd. water; elem. anal.;
DOI:10.1002/zaac.200600260