C₂₂H₂₂N₂O₅

Base Information

Chemical Name:C₂₂H₂₂N₂O₅
CAS No.:1036390-68-7
Molecular Formula:C₂₂H₂₂N₂O₅
Molecular Weight:394.427
Hs Code.:

C<sub>22</sub>H<sub>22</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₂N₂O₅

Chemical Property:

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Technology Process of C₂₂H₂₂N₂O₅

There total 8 articles about C₂₂H₂₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1036390-68-7
C₂₂H₂₂N₂O₅

Guidance literature:

Reference yield:

: 1975-52-6
5-nitro-o-toluic acid

: 1036390-68-7
C₂₂H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 80 °C / Inert atmosphere

2: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3: neat (no solvent) / 115 °C / Inert atmosphere

4: ammonia / ethylene glycol / 150 °C / Microwave irradiation

5: N-Bromosuccinimide / N,N-dimethyl acetamide / 0.17 h / 200 °C / Microwave irradiation

6: potassium phosphate; tricyclohexylphosphine; palladium diacetate / water; toluene / 0.17 h / 140 °C / Inert atmosphere; Microwave irradiation

7: hydrogen; palladium 10% on activated carbon / water; tetrahydrofuran / 3 h / 1034.32 Torr

8: N,N-dimethyl-formamide; acetonitrile; water / Microwave irradiation; Heating

With potassium phosphate; N-Bromosuccinimide; thionyl chloride; palladium 10% on activated carbon; ammonia; hydrogen; palladium diacetate; N,N-dimethyl-formamide; tricyclohexylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; ethylene glycol; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/acsmedchemlett.6b00282

Reference yield:

: 64688-68-2
2-methyl-5-nitrobenzoyl chloride

: 1036390-68-7
C₂₂H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2: neat (no solvent) / 115 °C / Inert atmosphere

3: ammonia / ethylene glycol / 150 °C / Microwave irradiation

4: N-Bromosuccinimide / N,N-dimethyl acetamide / 0.17 h / 200 °C / Microwave irradiation

5: potassium phosphate; tricyclohexylphosphine; palladium diacetate / water; toluene / 0.17 h / 140 °C / Inert atmosphere; Microwave irradiation

6: hydrogen; palladium 10% on activated carbon / water; tetrahydrofuran / 3 h / 1034.32 Torr

7: N,N-dimethyl-formamide; acetonitrile; water / Microwave irradiation; Heating

With potassium phosphate; N-Bromosuccinimide; palladium 10% on activated carbon; ammonia; hydrogen; palladium diacetate; tricyclohexylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; ethylene glycol; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/acsmedchemlett.6b00282