(W((C(CH₃)CHC(CH₃)CHC(CH₃)C)Se)3)2

Base Information

Chemical Name:(W((C(CH₃)CHC(CH₃)CHC(CH₃)C)Se)3)2
CAS No.:129321-16-0
Molecular Formula:C₅₄H₆₆Se₆W₂
Molecular Weight:1556.58
Hs Code.:

(W((C(CH<sub>3</sub>)CHC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)C)Se)3)2

Synonyms:

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Chemical Property of (W((C(CH₃)CHC(CH₃)CHC(CH₃)C)Se)3)2

Chemical Property:

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Technology Process of (W((C(CH₃)CHC(CH₃)CHC(CH₃)C)Se)3)2

There total 2 articles about (W((C(CH₃)CHC(CH₃)CHC(CH₃)C)Se)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.3%

: 54935-70-5
hexakis(dimethylamido)ditungsten(III)

: 55560-58-2
2,4,6-Trimethylbenzeneselenol

: 129321-16-0
(W((C(CH₃)CHC(CH₃)CHC(CH₃)C)Se)3)2

Guidance literature:: In toluene; byproducts: HNMe2; under N2, W2(NMe2)6 dissolved in toluene at room temp., dropwise addn. of mesitylene selenol to the stirred soln., color changed from yellow to red, stirred for 5 min, stand at ambient temp. for 3 days, pptn. of dark red brown crystals; filtration, washed with hexane and THF, air dried; elem. anal.;
DOI:10.1016/S0277-5387(00)84205-9

Reference yield:

: 63301-81-5
1,2-W₂Cl₂(dimethylamido)4

: 55560-58-2
2,4,6-Trimethylbenzeneselenol

: 129321-16-0
(W((C(CH₃)CHC(CH₃)CHC(CH₃)C)Se)3)2

Guidance literature:: In toluene; A greater than six-fold excess of mesityl selenol is added to the soln. of the tungsten chloro amide at room temp. The product is crystd. out from the soln. on standing for a few days.;
DOI:10.1039/C39900000920