C₂₆H₃₂O₆

Base Information

• Chemical Name: C₂₆H₃₂O₆
• CAS No.: 1462352-11-9
• Molecular Formula: C₂₆H₃₂O₆
• Molecular Weight: 440.536
• Mol file: 1462352-11-9.mol

Synonyms:

Chemical Property of C₂₆H₃₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₂O₆

There total 3 articles about C₂₆H₃₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

p-octyloxybenzoic acid (2493-84-7) + ethyl (4-hydroxybenzoyl)acetate (77103-47-0) → C26H32O6 (1462352-11-9)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 25h;

DOI:10.1134/S1070363213080148

Reference yield:

4-acetyloxy-benzoic acid (2345-34-8) → C26H32O6 (1462352-11-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: thionyl chloride

2.1: magnesium chloride; pyridine / dichloromethane / 5 °C

2.2: 20 °C / Cooling with ice

3.1: ammonium chloride; ammonia / ethanol; water / 4 h / 20 °C

4.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 25 h

With pyridine; dmap; thionyl chloride; ammonia; ammonium chloride; dicyclohexyl-carbodiimide; magnesium chloride; In ethanol; dichloromethane; water;

DOI:10.1134/S1070363213080148

Reference yield:

4-acetoxybenzoyl chloride (27914-73-4) → C26H32O6 (1462352-11-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: magnesium chloride; pyridine / dichloromethane / 5 °C

1.2: 20 °C / Cooling with ice

2.1: ammonium chloride; ammonia / ethanol; water / 4 h / 20 °C

3.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 25 h

With pyridine; dmap; ammonia; ammonium chloride; dicyclohexyl-carbodiimide; magnesium chloride; In ethanol; dichloromethane; water;

DOI:10.1134/S1070363213080148

upstream raw materials:

p-octyloxybenzoic acid

ethyl (4-hydroxybenzoyl)acetate

4-acetyloxy-benzoic acid

4-acetoxybenzoyl chloride

Refernces