C₃₀H₃₃F₉N₆O₂

Base Information

Chemical Name:C₃₀H₃₃F₉N₆O₂
CAS No.:874502-20-2
Molecular Formula:C₃₀H₃₃F₉N₆O₂
Molecular Weight:680.617
Hs Code.:

C<sub>30</sub>H<sub>33</sub>F<sub>9</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₃₀H₃₃F₉N₆O₂

Chemical Property:

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Technology Process of C₃₀H₃₃F₉N₆O₂

There total 12 articles about C₃₀H₃₃F₉N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 474645-96-0
(2R,4S)-(2-ethyl-6-trifluoromethyl-1,2,3,4-tetrahydroquinolin-4-yl)carbamic acid benzyl ester

: 874502-20-2
C₃₀H₃₃F₉N₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 760.05 Torr

3: sodium tris(acetoxy)borohydride; acetic acid / 1,1-dichloroethane / 20 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

5: sodium azide; triethylamine / toluene / 110 °C

6: triphenylphosphine

With pyridine; sodium azide; sodium tris(acetoxy)borohydride; palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; 1,1-dichloroethane; ethyl acetate; toluene; 6: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2012.04.042

Reference yield:

: 261947-57-3
[2R,4S]4-(3,5-bis-trifluoromethyl-benzylamino)-2-ethyl-6-trifluoromethyl-3,4-dihydro-2H-quinoline-1-carboxylic acid isopropyl ester

: 874502-20-2
C₃₀H₃₃F₉N₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

2: sodium azide; triethylamine / toluene / 110 °C

3: triphenylphosphine

With sodium azide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; toluene; 3: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2012.04.042

Reference yield:

: 98-56-6
4-chlorobenzotrifluoride

: 874502-20-2
C₃₀H₃₃F₉N₆O₂

Guidance literature:: Multi-step reaction with 10 steps

1: palladium diacetate; caesium carbonate; DavePhos; phenylboronic acid / dichloromethane; toluene / 80 °C

2: sulfuric acid / toluene / 35 °C

3: lithium tert-butoxide / tetrahydrofuran; diethyl ether / -10 - 0 °C

4: sodium tetrahydroborate; magnesium chloride / ethanol; water

5: pyridine / 0 - 20 °C

6: palladium 10% on activated carbon; hydrogen / ethyl acetate / 760.05 Torr

7: sodium tris(acetoxy)borohydride; acetic acid / 1,1-dichloroethane / 20 °C

8: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

9: sodium azide; triethylamine / toluene / 110 °C

10: triphenylphosphine

With pyridine; sodium tetrahydroborate; sodium azide; sodium tris(acetoxy)borohydride; sulfuric acid; palladium 10% on activated carbon; hydrogen; palladium diacetate; caesium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; magnesium chloride; lithium tert-butoxide; DavePhos; phenylboronic acid; In tetrahydrofuran; diethyl ether; 1,1-dichloroethane; ethanol; dichloromethane; water; ethyl acetate; toluene; 10: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2012.04.042