Technology Process of C36H50O6Si
There total 25 articles about C36H50O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) phenylselenyl chloride, triethylamine, 2.) sodium metaperiodate, sodium bicarbonate, 2.) calcium carbonate
2: 1.) hydroxytating agent
3: imidazole / dimethylformamide
4: acetonitrile / 10 h / 170 °C
With
1H-imidazole; sodium periodate; Phenylselenyl chloride; hydroxytating agent; sodium hydrogencarbonate; triethylamine; calcium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00541a044
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) phenylselenyl chloride, triethylamine, 2.) sodium metaperiodate, sodium bicarbonate, 2.) calcium carbonate
2: 1.) hydroxytating agent
3: imidazole / dimethylformamide
4: acetonitrile / 10 h / 170 °C
With
1H-imidazole; sodium periodate; Phenylselenyl chloride; hydroxytating agent; sodium hydrogencarbonate; triethylamine; calcium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00541a044
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) acid, 2.) methanesulfonyl chloride, triethylamine / 2.) methylene chloride
2: 1.) phenylselenyl chloride, triethylamine, 2.) sodium metaperiodate, sodium bicarbonate, 2.) calcium carbonate
3: 1.) hydroxytating agent
4: imidazole / dimethylformamide
5: acetonitrile / 10 h / 170 °C
With
1H-imidazole; sodium periodate; Phenylselenyl chloride; hydroxytating agent; sodium hydrogencarbonate; methanesulfonyl chloride; triethylamine; calcium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00541a044