Thiophen-2-yl-(4,4,7-trimethyl-1-sulfanylidenedithiolo[3,4-c]quinolin-5-yl)methanone

Base Information

Chemical Name:Thiophen-2-yl-(4,4,7-trimethyl-1-sulfanylidenedithiolo[3,4-c]quinolin-5-yl)methanone
CAS No.:4595-67-9
Molecular Formula:C₈H₅BrN₂S
Molecular Weight:241.111
Hs Code.:
DSSTox Substance ID:DTXSID80360336
Wikidata:Q82142021

Synonyms:4595-67-9;thiophen-2-yl-(4,4,7-trimethyl-1-sulfanylidenedithiolo[3,4-c]quinolin-5-yl)methanone;DTXSID80360336;STL361108;AKOS000645359;thiophen-2-yl(4,4,7-trimethyl-1-thioxo-1,4-dihydro-5H-[1,2]dithiolo[3,4-c]quinolin-5-yl)methanone

Suppliers and Price of Thiophen-2-yl-(4,4,7-trimethyl-1-sulfanylidenedithiolo[3,4-c]quinolin-5-yl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Thiophen-2-yl-(4,4,7-trimethyl-1-sulfanylidenedithiolo[3,4-c]quinolin-5-yl)methanone

Chemical Property:

Vapor Pressure:6.82E-14mmHg at 25°C
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:389.00364880
Heavy Atom Count:24
Complexity:614

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)C3=C(C(N2C(=O)C4=CC=CS4)(C)C)SSC3=S

Technology Process of Thiophen-2-yl-(4,4,7-trimethyl-1-sulfanylidenedithiolo[3,4-c]quinolin-5-yl)methanone

There total 2 articles about Thiophen-2-yl-(4,4,7-trimethyl-1-sulfanylidenedithiolo[3,4-c]quinolin-5-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3437-95-4,149762-92-5
2-Iodothiophene

: 4595-60-2
2-bromopyrimidine

: 4595-67-9
4--2-brom-pyrimidin

Guidance literature:: 2-bromopyrimidine; With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran; at -60 ℃; for 1.5h; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; at -60 - 25 ℃; for 3h; Inert atmosphere;

2-Iodothiophene; With trifuran-2-yl-phosphane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 0.5h; regioselective reaction; Inert atmosphere;
DOI:10.1055/s-0028-1083208