C₂₁H₂₂N₂O₆S

Base Information

Chemical Name:C₂₁H₂₂N₂O₆S
CAS No.:1411995-68-0
Molecular Formula:C₂₁H₂₂N₂O₆S
Molecular Weight:430.481
Hs Code.:

C<sub>21</sub>H<sub>22</sub>N<sub>2</sub>O<sub>6</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₂N₂O₆S

Chemical Property:

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Technology Process of C₂₁H₂₂N₂O₆S

There total 4 articles about C₂₁H₂₂N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1411995-69-1
C₂₃H₂₈N₂O₇S

: 1411995-68-0
C₂₁H₂₂N₂O₆S

Guidance literature:: With lithium iodide; In pyridine; for 96h; Reflux;
DOI:10.1016/j.bmcl.2012.10.003

Reference yield:

: 2735-04-8,161687-55-4
2,4-Dimethoxyaniline

: 1411995-68-0
C₂₁H₂₂N₂O₆S

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 4 h / 20 °C

2: chlorosulfonic acid / 48 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 60 °C

4: hydrogenchloride / ethanol; water / 80 °C

5: N-ethyl-N,N-diisopropylamine; HATU

6: lithium iodide / pyridine / 96 h / Reflux

With pyridine; hydrogenchloride; chlorosulfonic acid; N-ethyl-N,N-diisopropylamine; HATU; lithium iodide; In pyridine; ethanol; water; acetonitrile;
DOI:10.1016/j.bmcl.2012.10.003

Reference yield:

: 5-acetylamino-2,4-dimethoxy-benzenesulfonyl chloride

: 1411995-68-0
C₂₁H₂₂N₂O₆S

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 60 °C

2: hydrogenchloride / ethanol; water / 80 °C

3: N-ethyl-N,N-diisopropylamine; HATU

4: lithium iodide / pyridine / 96 h / Reflux

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; HATU; lithium iodide; In pyridine; ethanol; water; acetonitrile;
DOI:10.1016/j.bmcl.2012.10.003